CasNo： 54197-66-9
MF： C9H9NO2
Appearance： Off-white solid
InChI:InChI=1/C9H9NO2/c11-7-2-3-8-6(5-7)1-4-9(12)10-8/h2-3,5,11H,1,4H2,(H,10,12)
HCl is added to the reaction solvent N, ...
Tetrahydroquinoline, quinoline, and dihy...
The invention belongs to the field of pr...
The invention provides a synthesis metho...
N-(4-methoxyphenyl)-β-chloropropanamide
3,4-dihydro-6-hydroxy-2(1H)-quinolinone
| Conditions | Yield |
|---|---|
|
With
palladium dichloride;
In
tetrahydrofuran;
at 100 - 110 ℃;
for 3h;
|
95% |
|
With
aluminum (III) chloride;
In
N,N-dimethyl acetamide;
at 150 ℃;
for 2h;
Temperature;
Solvent;
Concentration;
|
86.5% |
|
With
hydrogenchloride; aluminum (III) chloride; triethylamine hydrochloride;
In
n-heptane; N,N-dimethyl acetamide;
at 25 ℃;
for 1h;
Ionic liquid;
Inert atmosphere;
|
86.2% |
|
With
aluminium trichloride;
In
chlorobenzene;
at 120 ℃;
for 6h;
|
4% |
|
With
aluminum (III) chloride;
at 150 ℃;
|
|
|
With
aluminum (III) chloride;
In
N,N-dimethyl acetamide;
at 140 - 150 ℃;
|
3-chloro-propionic acid p-phenetidide
3,4-dihydro-6-hydroxy-2(1H)-quinolinone
| Conditions | Yield |
|---|---|
|
With
palladium dichloride;
In
tetrahydrofuran;
at 100 - 110 ℃;
for 3h;
|
87% |
|
With
aluminium trichloride;
durch Schmelzen;
|
3-chloro-propionic acid-(4-hydroxy-anilide)
3-chloro-propionic acid p-phenetidide
N-methoxy-3,4-dihydro-1H-quinolin-2-one
N-(4-methoxyphenyl)-β-chloropropanamide
6-[3-(1-Phenyltetrazol-5-yl)propoxy]-3,4-dihydrocarbostyril
6-<3-(1-cyclohexyl-5-tetrazolyl)propoxy>-2-oxo-1,2,3,4-tetrahydroquinoline
6-[3-(1-Cyclohexylmethyltetrazol-5-yl)propoxy]-3,4-dihydrocarbostyril
6-[5-(1-Cyclohexyl-1H-tetrazol-5-yl)-pentyloxy]-3,4-dihydro-1H-quinolin-2-one
