CasNo： 100516-88-9
MF： C10H9NO
Appearance： pink solid
InChI:InChI=1/C10H9NO/c12-7-8-3-4-10-9(6-8)2-1-5-11-10/h1-6,12H,7H2
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2-Methyl-benzoic acid quinolin-6-ylmethyl ester
ortho-methylbenzoic acid
6-(hydroxymethyl)quinoline
| Conditions | Yield |
|---|---|
|
With
water in alkaline medium;
In
acetone;
Rate constant;
Ambient temperature;
|
6-(methoxycarbonyl)quinoline
6-(hydroxymethyl)quinoline
| Conditions | Yield |
|---|---|
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at -20 ℃;
for 1h;
|
94% |
|
With
diisobutylaluminium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
|
93% |
|
6-(methoxycarbonyl)quinoline;
With
diisobutylaluminium hydride;
In
tetrahydrofuran;
at -78 - 0 ℃;
for 1h;
Cooling with acetone-dry ice;
With
methanol; acetic acid;
In
tetrahydrofuran;
for 0.0833333h;
With
water; sodium tartrate;
In
tetrahydrofuran;
for 0.333333h;
|
93% |
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at -20 ℃;
for 1h;
|
85% |
|
With
diisobutylaluminium hydride;
In
dichloromethane;
at 0 - 20 ℃;
|
65% |
|
6-(methoxycarbonyl)quinoline;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
With
water; sodium hydroxide;
In
tetrahydrofuran;
for 0.333333h;
|
64% |
|
6-(methoxycarbonyl)quinoline;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 ℃;
for 0.333333h;
With
sodium hydroxide;
In
tetrahydrofuran; water;
for 0.333333h;
|
64% |
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
|
51% |
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 5h;
|
|
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 5h;
|
|
|
With
diisobutylaluminium hydride;
In
diethyl ether; toluene;
at -70 - 20 ℃;
|
quinoline-6-carbaldehyde
quinoline-6-carboxylic acid ethyl ester
2-Methyl-benzoic acid quinolin-6-ylmethyl ester
6-(methoxycarbonyl)quinoline
6-(chloromethyl)quinoline
6-bromomethyl quinoline
6-iodomethyl-quinoline
2-(quinolin-6-yl)acetonitrile
